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Novel side chain modified Δ8(14)-15-ketosterols

✍ Scribed by Alexander Yu. Misharin; Vitali S. Ivanov; Arif R. Mehtiev; Galina E. Morozevich; Yaroslav V. Tkachev; Vladimir P. Timofeev

Book ID
116892026
Publisher
Elsevier Science
Year
2007
Tongue
English
Weight
335 KB
Volume
72
Category
Article
ISSN
0039-128X

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✍ Abdul U. Siddiqui; William K. Wilson; George J. Schroepfer Jr. 📂 Article 📅 1994 🏛 Elsevier Science 🌐 English ⚖ 879 KB

25R)-3/3,26-Dihydroxy-5c~-cholest-8( 14)-en-15-one (1) was synthesized in four steps from (25R)-3/3,26-diacetoxycholesta-5,7-diene (111) in 30% overall yield, lsomerization of 111 with HCI in chloroform-dichloromethane at -60°C gave (25R)-3/3,26-diacetoxy-5et-cholesta-7,14-diene together with the 5u