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Novel pyrazole functionalized phthalocyanines and their first row transition metal complexes

✍ Scribed by Dehe, Daniel; Lothschütz, Christian; Thiel, Werner R.

Book ID
121370763
Publisher
Royal Society of Chemistry
Year
2010
Tongue
English
Weight
723 KB
Volume
34
Category
Article
ISSN
1144-0546

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✍ Germund Glatz; Serhiy Demeshko; Günter Motz; Rhett Kempe 📂 Article 📅 2009 🏛 John Wiley and Sons 🌐 English ⚖ 305 KB

## Abstract Lithiated 4‐methyl‐2‐[(trimethylsilyl)amino]pyridine (Ap^TMS^H) undergoes a salt metathesis reaction with [ScCl~3~(thf)~3~] and FeCl~3~, at low temperature in thf, to yield the homoleptic complexes [Sc(Ap^TMS^)~3~] (1) and [Fe(Ap^TMS^)~3~] (2). An analogous reaction with MnCl~2~, CoCl~2