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Novel (4-Piperidin-1-yl)-phenyl Sulfonamides as Potent and Selective Human β3 Agonists

✍ Scribed by Baihua Hu; John Ellingboe; Stella Han; Elwood Largis; Kitae Lim; Michael Malamas; Ruth Mulvey; Chuansheng Niu; Alexander Oliphant; Jeffrey Pelletier; Thiruvikraman Singanallore; Fuk-Wah Sum; Jeff Tillett; Victoria Wong

Book ID: 108479084
Publisher: Elsevier Science
Year: 2001
Tongue: English
Weight: 326 KB
Volume: 9
Category: Article
ISSN: 0968-0896
DOI: 10.1016/s0968-0896(01)00114-6

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## Abstract For Abstract see ChemInform Abstract in Full Text.

ChemInform Abstract: 2,4-Thiazolidinedio

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Scheme 1. Reagents and conditions: a) NaH, DMF (anhyd), RT; b) CH 3 OH (anhyd), reflux; c) di-tert-butyldicarbonate, CH 2 Cl 2 , RT; d) H 2 (10 atm), 20 % Pd(OH) 2 /C, EtOAc, RT; e) HSO 3 Cl, 0 8C; f) CH 2 Cl 2 , RT. Scheme 2. Reagents and conditions: a) TFA in CH 2 Cl 2 , 08C; b) 1 n NaOH, THF, RT