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Notes- The Anomalous Diels-Alder Reaction of 2,3-Dicyano-p-benzoquinone with 1,2-Dimethylenecyclobutane

✍ Scribed by Hartzler, H; Benson, R

Book ID
126929395
Publisher
American Chemical Society
Year
1961
Tongue
English
Weight
121 KB
Volume
26
Category
Article
ISSN
0022-3263

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Diels-Alder cycloaddition of cyclopentadiene (1) to 2,3-dicyano-p-benzoquinone (2), when performed in methanol solvent at ambient temperature (kinetic control), gave 3b. Reduction of 3b, carried out under mild conditions by using CeCI3-NaBH4, proceeded stereospecifically to afford diol $. Subsequent