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Nonradical tetrabutylammonium monopersulfate oxidation of hydrocarbons catalyzed by [Mn3O4bipy4(H2O)2](ClO4)4

✍ Scribed by Jeremy Wessel; Robert H. Crabtree

Publisher
Elsevier Science
Year
1996
Tongue
English
Weight
855 KB
Volume
113
Category
Article
ISSN
1381-1169

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Single crystals of Lu(ClO 4 ) 3 Β΄3 H 2 O were obtained by slow dehydration of Lu(ClO 4 ) 3 Β΄6 H 2 O at 140 Β°C under flowing argon. The compound crystallizes in the triclinic crystal system (P1, Z = 2, a = 750.3(1), b = 838.4(1), c = 1054.6(2) pm, a = 79.77(2)Β°, b = 79.18(2), c = 63.83(2), R all = 0.