The title compound, C 14 H 17 NO 2 , crystallizes with four independent molecules (A, B, C and D) in the asymmetric unit. In the crystal structure, molecules A and C are hydrogen bonded to their symmetry-related molecules to form parallel chains extending in the a direction. Molecules B and D are hy
N,N-Dimethyl-5-[2-(hydroxymethyl)-4-nitrophenyl]pent-4-ynamide
✍ Scribed by Bats, Jan W. ;Schäfer, Sascha ;Hashmi, A. Stephen K.
- Publisher
- International Union of Crystallography
- Year
- 2006
- Tongue
- English
- Weight
- 317 KB
- Volume
- 62
- Category
- Article
- ISSN
- 1600-5368
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The title compound, C 18 H 20 ClN 3 O 2 , is a potent new herbicide. X-ray analysis reveals that the benzene ring is twisted away from the isoxazole ring by 67.7 (1) . The crystal packing is stabilized by intermolecular N-HÁ Á ÁN and C-HÁ Á ÁO hydrogen bonds.
In the title compound, two aromatic rings are almost perpendicular to each other with a dihedral angle of 72.4 (1) .
The title compound, C 23 H 26 BrN 5 O 2 , was synthesized by the reaction of 4- [(2,6-dimethylphenyl)aminocarbonylmethyl]piperazine and 3-(3-nitrophenyl)-5-chloromethyl-1,2,4-oxadiazole. There are intramolecular C-HÁ Á ÁN and intermolecular N-HÁ Á ÁO and C-HÁ Á ÁO hydrogen bonds in the crystal struc
The title compound, C 23 H 26 ClN 5 O 2 , was synthesized by the reaction of 4- [(2,6-dimethylphenyl)aminocarbonylmethyl]piperazine and 5-chloromethyl-3-(2-chlorophenyl)-1,2,4oxadiazole. In the structure, there are intramolecular C-HÁ Á ÁN, N-HÁ Á ÁN and C-HÁ Á ÁO hydrogen bonds, and intermolecular