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N,N-Dibenzyl­aniline

✍ Scribed by Bi, Quan-Xi ;Tong, Hong-Bo ;Zhou, Mei-Su

Publisher
International Union of Crystallography
Year
2007
Tongue
English
Weight
104 KB
Volume
63
Category
Article
ISSN
1600-5368

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A new polymorph of N,N-dibenzylaniline
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The title compound, C 20 H 19 N, is a second polymorph of N,Ndibenzylaniline [Bi, Tong & Zhou (2007). Acta Cryst. E63, o1809-o1810]. The present polymorph and that already reported crystallize in the monoclinic space group P2 1 /n with one and two independent molecules, respectively. The molecular c

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Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.008 A Ê R factor = 0.046 wR factor = 0.117 Data-to-parameter ratio = 12.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

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## Partie expe Ârimentale Le N-(2-bromoe  thyl)-N H ,N H -dibenzylsulfamide est obtenu a Á la ®n des trois re  actions en chaõ Ãne suivantes:

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N,N-dibe3rzyl-2-amh30propamd la daived from alanine rearrangesto the cormaponding ketone,NJ%tibenzyl-1-aminopropanone uponexpmuretoeirher silieagelor pyridhrimnacetate. Simitar rearmngemenrado not occur with aldebydes&aivedfrom phenytafinhte, valirre, leueine, prolineor phenylglycirre. Ooe meeharris