Single-crystal X-ray study T = 273 K Mean '(C±C) = 0.002 A Ê R factor = 0.038 wR factor = 0.110 Data-to-parameter ratio = 15.0 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
N,N′-Di-o-tolylthiourea
✍ Scribed by Kuan, Fong Sheen ;Tiekink, Edward R. T.
- Book ID
- 104492490
- Publisher
- International Union of Crystallography
- Year
- 2007
- Tongue
- English
- Weight
- 410 KB
- Volume
- 63
- Category
- Article
- ISSN
- 1600-5368
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✦ Synopsis
Two independent molecules comprise the asymmetric unit in the title compound, C 15 H 16 N 2 S. These are connected into a dimer via an eight-membered thioamide {Á Á ÁH-N-C S} 2 synthon. Interactions of the type N-HÁ Á Á and C-HÁ Á Á consolidate molecules into a layer structure.
📜 SIMILAR VOLUMES
## The title compounds Zn 2 )] 2 3 build mixed crystals in the ratio 0.42 : 0.58. Each compound forms dimers, in which the monomer moieties are related via a two-fold axis, coinciding with that of the monoclinic space group C2/c. The lattice parameters are a = 23.581( ), b = 17.112(5), c = 16.372(