N,N′-Bis(tert-butoxycarbonyl)thiourea
✍ Scribed by Li, Cong ;Chan, Kannie Wai Yan ;Szeto, Lap
- Publisher
- International Union of Crystallography
- Year
- 2003
- Tongue
- English
- Weight
- 233 KB
- Volume
- 59
- Category
- Article
- ISSN
- 1600-5368
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✦ Synopsis
The title compound, C 11 H 20 O 4 N 2 S, has a planar skeleton and its crystal structure is stabilized by extensive intermolecular (NÐHÁ Á ÁS) and intramolecular (NÐHÁ Á ÁO and CÐHÁ Á ÁO) hydrogen-bonding interactions.
📜 SIMILAR VOLUMES
The title compound, C 10 H 12 N 2 O 2 S, adopts a cis±trans con®guration, where the phenyl group and the ethoxycarbonyl moiety lie, respectively, cis and trans relative to the S atom across the thiourea CÐN bonds. Both NÐH atoms participate in intermolecular hydrogen bonds and one also forms an intr
Single-crystal X-ray study T = 296 K Mean '(C±C) = 0.003 A Ê R factor = 0.042 wR factor = 0.115 Data-to-parameter ratio = 15.2 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
The structure of the title compound, C 17 H 20 N 2 S, exhibits hydrogen bonding of the type N-HÁ Á ÁS, resulting in chains of molecules running along the b axis.