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[N,N′-Bis(3-methyl­salicyl­idene)propane-1,3-diaminato]copper(II)

✍ Scribed by You, Zhong-Lu

Publisher
International Union of Crystallography
Year
2005
Tongue
English
Weight
108 KB
Volume
61
Category
Article
ISSN
1600-5368

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[N,N′-Bis(3-methyl­salicyl­idene)-1,3-pr
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✍ You, Zhong-Lu 📂 Article 📅 2005 🏛 International Union of Crystallography 🌐 English ⚖ 110 KB

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[N,N′-Bis­(salicyl­idene)-1,3-propane­diaminato](methanol)(thio­cyanato)­nickel(II)
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Single-crystal X-ray study T = 298 K Mean '(C±C) = 0.005 A Ê Disorder in main residue R factor = 0.036 wR factor = 0.107 Data-to-parameter ratio = 14.1 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

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Porous solvent-free μ2-bis­(salicyl­idene)propane-1,3-diaminato-bis­{[bis­(salicyl­idene)propane-1,3-diaminato]iron(III)}
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The title compound, [Fe 2 (C 17 H 16 N 2 O 2 ) 3 ], was isolated from the reaction between iron(III) perchlorate hydrate and a mixture of 1,3-bis(salicylideneamino)propane and triethylamine in ethanol. Recrystallization from a dichloroethane solution resulted in a porous solvent-free array of molecu