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N,N′-Bis(2-pyrid­yl)naphthalene-1,4-carboxamide

✍ Scribed by Jing, Lin-Hai ;Gu, Shao-Jin ;Zhang, Huan-Xia

Publisher
International Union of Crystallography
Year
2006
Tongue
English
Weight
98 KB
Volume
62
Category
Article
ISSN
1600-5368

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✦ Synopsis

The title compound, C 22 H 16 N 4 O 2 , crystallizes in an anti C O conformation. The two amide groups are twisted away from the attached ring by 69.94 (6) and 62.99 (7) . The crystal packing is stabilized by N-HÁ Á ÁN and C-HÁ Á ÁO hydrogen bonds, and also by C-HÁ Á Á interactions.

📜 SIMILAR VOLUMES

N,N′-Bis[2-(2-pyrid­yl)eth­yl]dithio­oxa
N,N′-Bis[2-(2-pyrid­yl)eth­yl]dithio­oxamide
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The title compound, C 16 H 18 N 4 S 2 , has a crystallographic inversion centre at the mid-point of the central C-C bond. The plane of the dithiooxamide fragment is approximately perpendicular to the plane of the dimethylene bridge [dihedral angle = 84.8 (1) ], the plane of which is in turn normal t

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Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.004 A Ê R factor = 0.043 wR factor = 0.104 Data-to-parameter ratio = 13.9 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

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✍ Hino, Kazuyuki ;Mizuguchi, Jin 📂 Article 📅 2005 🏛 International Union of Crystallography 🌐 English ⚖ 205 KB

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