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NMR-spektroskopische Untersuchungen an cyclischen Ketonen unter Anwendung von Tris(1,1,1,2,2,3,3,-heptafluoro-7,7-dimethyloctan-4,6-dionato)europium(III)

✍ Scribed by Horst Remane; Erich Kleinpeter; Rolf Borsdorf


Book ID
104609188
Publisher
Wiley (John Wiley & Sons)
Year
2010
Weight
231 KB
Volume
15
Category
Article
ISSN
0044-2402

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A simple, rapid, and quantitative NMR method was developed for the determination of the ratio of the diastereoisomers present in 7-chloro-3,3a-dihydro-2-methyl-2H, 9H-isoxazolo(3,2-b)(1,3)benzoxazin-9-one (I). Deuterated tris(1,1,1,2,2,3,3heptafluoro-7,7-dimethyl-4,6-octanedionato)europium I11 shift