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Nuclear magnetic resonance studies. III. Application of tris-(1,1,1,2,2,3,3-heptafluoro-7,7-Dimethyl-4,6-octanedionato)europium as a shift reagent for phenols

✍ Scribed by Liu Kwang-Ting; Hsu Min-Fu; Chen Jenn-Shing


Book ID
104244285
Publisher
Elsevier Science
Year
1974
Tongue
French
Weight
165 KB
Volume
15
Category
Article
ISSN
0040-4039

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✦ Synopsis


The application of @-diketone complexes of lanthanide ions as nmr shift reafents to many classes of organic compounds is a recent development of great potential and utility.

2 They were, however,


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NMR assay of diastereoisomers of 7-chlor
✍ Philip Reisberg; Ian A. Brenner; Jerome I. Bodin πŸ“‚ Article πŸ“… 1974 πŸ› John Wiley and Sons 🌐 English βš– 398 KB

A simple, rapid, and quantitative NMR method was developed for the determination of the ratio of the diastereoisomers present in 7-chloro-3,3a-dihydro-2-methyl-2H, 9H-isoxazolo(3,2-b)(1,3)benzoxazin-9-one (I). Deuterated tris(1,1,1,2,2,3,3heptafluoro-7,7-dimethyl-4,6-octanedionato)europium I11 shift