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NMR determination of enantiomers of 7-chloro-3,3a-dihydro-2-methyl-2H,9H-isoxazolo[3,2-b][1,3]benzoxazin-9-one using chiral shift reagent, tris[3-(heptafluorobutyryl)-d-camphorato]europium(III)

โœ Scribed by Philip Reisberg; Ian A. Brenner; Jerome I. Bodin

Publisher
John Wiley and Sons
Year
1976
Tongue
English
Weight
204 KB
Volume
65
Category
Article
ISSN
0022-3549

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A simple, rapid, and quantitative NMR method was developed for the determination of the ratio of the diastereoisomers present in 7-chloro-3,3a-dihydro-2-methyl-2H, 9H-isoxazolo(3,2-b)(1,3)benzoxazin-9-one (I). Deuterated tris(1,1,1,2,2,3,3heptafluoro-7,7-dimethyl-4,6-octanedionato)europium I11 shift

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