NMR analysis of a series of substituted pyrazolo[3,4-d] pyrimidines-4-amines
✍ Scribed by Lígia M. Rodrigues; Aravind Sivasubramanian; Elisa M. Pinto; Ana M. F. Oliveira-Campos; Julio A. Seijas; M. Pilar Vázquez-Tato
- Publisher
- John Wiley and Sons
- Year
- 2009
- Tongue
- English
- Weight
- 72 KB
- Volume
- 47
- Category
- Article
- ISSN
- 0749-1581
- DOI
- 10.1002/mrc.2329
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✦ Synopsis
Abstract
A series of 21 substituted pyrazolo[3,4‐d]pyrimidines‐4‐amines were studied by ^1^H and ^13^C NMR. The application of two‐dimensional techniques, HMQC and HMBC, allowed the complete assignment of the spectra for all the compounds. Copyright © 2008 John Wiley & Sons, Ltd.
📜 SIMILAR VOLUMES
## Abstract Pyrazolo‐[3,4‐__d__]pyrimidine‐4,6‐diones **5** and pyrazolo[4,3‐__d__]pyrimidine‐5,7‐diones **7** were synthesized by Curtius rearrangement of pyrazolic mono‐esters **2** and **3** followed by hetero‐cyclization __via__ the ureas derivatives **4** and **6** under alkaline conditions.
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