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Nitrosyl Azide, N4O, an Intrinsically Unstable Oxide of Nitrogen

✍ Scribed by Dipl.-Chem. Axel Schulz; Dr. Inis C. Tornieporth-Oetting; Priv.-Doz. Dr. Thomas M. Klapötke

Publisher
John Wiley and Sons
Year
1993
Tongue
English
Weight
388 KB
Volume
32
Category
Article
ISSN
0044-8249

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✍ Elisabeth Irran; Klaus Köllisch; Stefano Leoni; Reinhard Nesper; Paul F. Henry; 📂 Article 📅 2000 🏛 John Wiley and Sons 🌐 English ⚖ 322 KB

The yellow-orange oxonitridosilicate oxide Ce 4 [Si 4 O 4 N 6 ]O was obtained by the reaction of cerium metal with Si(NH) 2 and SiO 2 in a radiofrequency furnace at 1560 8C. The crystal structure was determined by single-crystal X-ray diffraction (a 1033.67(6) pm, P2 1 3, Z 4, R1 0.0412, wR2 0.0678)