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Nickelkatalysierte Cyclodimerisation von 2-tert-Butyl- und 2-Trimethylsilyl-1,3-butadien

✍ Scribed by Dr. Tamas Bartik; Prof. Paul Heimbach; Thomas Himmler; Dr. Richard Mynott

Publisher
John Wiley and Sons
Year
1985
Tongue
English
Weight
220 KB
Volume
97
Category
Article
ISSN
0044-8249

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πŸ“œ SIMILAR VOLUMES

Nickel-Catalyzed Cyclodimerization of 2-
Nickel-Catalyzed Cyclodimerization of 2-tert-Butyl- and 2-Trimethylsilyl-1,3-butadiene
✍ Dr. Tamas Bartik; Prof. Paul Heimbach; Dipl.-Chem. Thomas Himmler; Dr. Richard M πŸ“‚ Article πŸ“… 1985 πŸ› John Wiley and Sons 🌐 English βš– 220 KB

161 16 g Al powder, suspended in 500 mL n-heptane, was treated for 4 d with C :Hr ( I bar) after addition of 30 g AICI, with stirring at 100Β°C. The mixture was filtered and the filtrate freed of solvent (maximum 50Β°C. 10mbar). The oily residue (17.75 g) was treated with pentane. A colorless powder p