Synthesis of 4-hydroxy[phenyl-U-14C]coum
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Allan K. Nadian
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Article
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1984
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John Wiley and Sons
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French
β 229 KB
## Abstract Radiolabeled 4βhydroxycoumarin was synthesized on a microscale by condensing [Uβ^14^C]phenol and malonic acid in the presence of anhydrous zinc chloride and phosphorus oxychloride. The yield was 14% on a 0.5 mmol scale at a specific activity of 107 ΞΌCi/mmol.