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New reaction of trithioorthoacetates. Reaction with acylating reagents

โœ Scribed by Hojo, Masaru; Masuda, Ryoichi

Book ID
120604719
Publisher
American Chemical Society
Year
1975
Tongue
English
Weight
417 KB
Volume
40
Category
Article
ISSN
0022-3263

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New reaction of trithioorthoacetates. Re
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โœ Hojo, Masaru; Masuda, Ryoichi ๐Ÿ“‚ Article ๐Ÿ“… 1975 ๐Ÿ› American Chemical Society ๐ŸŒ English โš– 417 KB

by preparing and chromatographing samples of the dinitrophenylhydrazones. Fractional crystallization of the crude mixture of 2,4-dinitrophenylhydrazones from ethanol gave a sample (mp 131-132') which did not depress the melting point of a known sample of cyclopropylacetaldehyde 2,4-dinitrophenylhydr

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Reactions between Tebbe reagent and acyl chlorides proceeded in non-Wittig type manner, giving the corresponding methyl ketones. A possible reaction mechanism is discussed. Recently, biscyclopentadienyl titanium-p-chloro-p-methylidene bismethyl aluminum 1 ( Tebbe reagent ) and its aluminum free ana