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New pulse sequence for long-range two-dimesional heteronuclear NMR chemical shift correlation

✍ Scribed by Andrew S. Zektzer; Michael J. Quast; Gary S. Linz; Gary E. Martin; J. Dew McKenney; Milton D. Johnston Jr; Raymond N. Castle

Publisher
John Wiley and Sons
Year
1986
Tongue
English
Weight
758 KB
Volume
24
Category
Article
ISSN
0749-1581

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✦ Synopsis

Techniques available for long-range heteronuclear chemical shift correlation are briefly reviewed. A new pulse sequence for long-range heteronuclear chemical shift correlation is described. Comparison of the results obtained using the new pulse sequence with those from conventional long-range optimized heteronuclear chemical shift correlation is presented. Total Assignments of the 'H and 13C NMR spectra of l-benzothieno[2,3-~lquinoline, the model compound used for the study, are reported.

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