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New process of preparation, structure, and physicochemical investigations of the new titanyl phosphate Ti2O(H2O)(PO4)2

✍ Scribed by S. Benmokhtar; A. El jazouli; J.P. Chaminade; P. Gravereau; M. Ménétrier; F. Bourée


Book ID
108195542
Publisher
Elsevier Science
Year
2007
Tongue
English
Weight
785 KB
Volume
180
Category
Article
ISSN
0022-4596

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Single crystals of sodium iron hydrogen phosphate, NaFe(HPO 4 )(H 2 PO 4 ) 2 ´H2 O, were prepared hydrothermally by heating a mixture of Fe 2 O 3 , H 3 PO 4 and Na 2 CO 3 with a small amount of water. It crystallizes orthorhombic (Pbcn (N°60), Z = 8, a = 872.91( 7), b = 1249.54(8), c = 1894.4(1) pm)