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New ionic fluorenylnickel complexes: Synthesis and solid state structure

✍ Scribed by Kozioł, Andrzej; Jerzykiewicz, Lucjan B.; Justyniak, Iwona; Lis, Tadeusz; Pasynkiewicz, Stanisław; Pietrzykowski, Antoni

Book ID
124105230
Publisher
Elsevier Science
Year
2014
Tongue
English
Weight
816 KB
Volume
767
Category
Article
ISSN
0022-328X

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Treatment of Ti(NtBu)Cl 2 (py) 2 (1, py = pyridine) with bulky stitution products [PhC(NiPr) 2 ] 2 Ti(NtBu)(py) (6) and [Ph 2 P(NSiMe 3 ) 2 ] 2 Ti(NtBu) (7). The bis(pyridine) adduct heteroallylic ligands in a 1:1 molar ratio affords the monosubstituted derivatives [PhC(NSiMe 3 ) 2 ]Ti(NtBu)Cl(py) 2