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New Fluorous Reversed Phase Silica Gels for HPLC Separations of Perfluorinated Compounds

โœ Scribed by H. Glatz; C. Blay; H. Engelhardt; W. Bannwarth

Book ID
111788087
Publisher
Springer
Year
2004
Tongue
English
Weight
269 KB
Volume
59
Category
Article
ISSN
0009-5893

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Synthesis of perfluorinated allylic comp
Synthesis of perfluorinated allylic compounds by radical allylation and their purification over fluorous reverse-phase silica
โœ Ilhyong Ryu; Sergio Kreimerman; Tatsuro Niguma; Satoshi Minakata; Mitsuo Komatsu ๐Ÿ“‚ Article ๐Ÿ“… 2001 ๐Ÿ› Elsevier Science ๐ŸŒ French โš– 62 KB

A simple free-radical method for the preparation of a variety of perfluorinated allylic compounds has been developed starting from perfluoroalkyl iodides and allyltins. Allyltributyltin, methallyltributyltin and crotyltributyltin all proved to be useful for the transformation. The desired perfluorin