New dideutero-perfluoroalkylated oligopeptide derivatives for protein-sequencing by gas chromatography-mass spectrometry
โ Scribed by H. Nau
- Book ID
- 119405412
- Publisher
- Elsevier Science
- Year
- 1974
- Tongue
- English
- Weight
- 344 KB
- Volume
- 59
- Category
- Article
- ISSN
- 0006-291X
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Trimethylsilyl derivatives of the alkylphosphonates and of certain aminoalkylphosphonates were found to be satisfactory for the characterization of these phosphorus compounds by gas chrom'atography and gas chromatography-mass spectrometry. The trimethylsilyl derivatives of the I-aminoalkylphosphonat
The mass spectra of the 0-trimethylsilylated trifluoro-dideuteroethyl polyamino alcohols, produced by LiAID,-reduction and 0-trimethylsilylation of Ntrifluororacetyl oligopeptide methyl esters, are evaluated. Characteristic mass spectra of derivatives are shown which are derived from peptides contai