New 1H-1-alkyl-6-methyl-3-phenyl-7-phenylazo-pyrazolo[5,1-c][1,2,4]triazoles through regioselective alkylation of 1H-6-methyl-3-phenyl-7-phenylazopyrazolo[5,1-c][1,2,4]triazoles
✍ Scribed by Bercean, Vasile-Nicolae ;Badea, Valentin ;Deleanu, Călin ;Nicolescu, Alina
- Book ID
- 111488330
- Publisher
- Walter de Gruyter GmbH
- Year
- 2012
- Tongue
- English
- Weight
- 316 KB
- Volume
- 10
- Category
- Article
- ISSN
- 2391-5420
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📜 SIMILAR VOLUMES
Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.005 A Ê R factor = 0.051 wR factor = 0.141 Data-to-parameter ratio = 14.9 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
Single-crystal X-ray study T = 295 K Mean '(C±C) = 0.003 A Ê R factor = 0.034 wR factor = 0.084 Data-to-parameter ratio = 12.8 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
In the molecule of the title compound, C 9 H 9 N 3 O, the dihedral angle between the planar rings is 7.49 (3) . In the crystal structure, intermolecular N-HÁ Á ÁO hydrogen bonds link the molecules into dimers, which may be effective in the stabilization of the crystal structure.
In the title compound, C 11 H 9 N 5 OS, the molecules are linked into chains along the c axis via N-HÁ Á ÁN hydrogen bonds. The packing is further stabilized by C-HÁ Á Á andinteractions.