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New 15- and 18-Membered Polyunsaturated Macrocyclic Silicohydrocarbons

✍ Scribed by O. G. Yarosh; V. V. Bystrova; A. I. Albanov; L. V. Klyba; M. G. Voronkov

Book ID
110327354
Publisher
Springer
Year
2001
Tongue
English
Weight
37 KB
Volume
71
Category
Article
ISSN
1070-3632

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Synthesis of 15- and 18-membered polythi
Synthesis of 15- and 18-membered polythiamacrocylic ligands
✍ V. V. Pavlishchuk; P. E. Strizhak πŸ“‚ Article πŸ“… 1989 πŸ› Springer US 🌐 English βš– 216 KB

Reaction of 1,8-dimercapto-3,6-dithioactane with oxa-, aza-, and thiadihaloderivatives under high dilution conditions in the presence of cesium carbonate, which acts as a template for the condensation reaction, produces 15-and 18-membered polythiamacrocyclic ligands in yields greater than 50%. Poly