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Nb6Se20Br6, a pseudo one-dimensional compound with a waved chain structure

โœ Scribed by A. Meerschaut; P. Grenouilleau; J. Rouxel

Publisher
Elsevier Science
Year
1986
Tongue
English
Weight
556 KB
Volume
61
Category
Article
ISSN
0022-4596

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Syntesis and Crystal Structure of Cs2Nb6
Syntesis and Crystal Structure of Cs2Nb6Br5F12: A Nb6 Cluster Compound with a One-Dimensional Nb6Bri5Fi7Fa6 Unit Connection
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The synthesis and the crystal structure of Cs 2 Nb 6 Br 5 F 12 containing octahedral niobium clusters are presented in this work. This bromo6uoride is based on a Nb 6 L i 12 F a 6 (L : Br and F) unit and crystallizes in the orthorhombic system (space group, Cccm; Z : 4; a : 9.2446(2) A s , b : 13.62

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Synthesis of the One-dimensional Compound (Ph4P)[In(P2Se6)] in a Ph4P+-Containing Selenophosphate Flux, and Structure of [In(P2Se6)2]5โ€“ โ€“ a Discrete Molecular Fragment of the [In(P2Se6)]nnโ€“ Chain
โœ Konstantinos Chondroudis; Debojit Chakrabarty; Enos A. Axtell; Mercouri G. Kanat ๐Ÿ“‚ Article ๐Ÿ“… 1998 ๐Ÿ› John Wiley and Sons ๐ŸŒ German โš– 137 KB ๐Ÿ‘ 2 views

The reaction of one equivalent of In with a molten flux of (Ph 4 P) 2 Se 5 and P 2 Se 5 (1 : 2), at 250 ยฐC gave the (Ph 4 P)[In(P 2 Se 6 )] (I). Stoichiometric elemental synthesis at 750 ยฐC produced the Cs 5 In(P 2 Se 6 ) 2 (II). The thin, yellow crystals of (I), and the irregular, dark orange cryst