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Naphtho[1,2-c:5,6-c]difuran: A Reactive Linker and Cyclophane Precursor.

✍ Scribed by Michelle E. Thibault; Taunia L. L. Closson; Sidney C. Manning; Peter W. Dibble

Publisher
John Wiley and Sons
Year
2004
Weight
56 KB
Volume
35
Category
Article
ISSN
0931-7597

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The title compound, an interesting analog of isobenzofuran, was prepared in nine steps from 2,6-dimethylnaphthalene in an overall yield of 12%.

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## Abstract The assignment of the NMR spectra of the polynuclear heteroaromatic naphtho[2′,1′:5,6]naphtho‐[2′,1′:4,5]thieno[2,3‐c]quinoline is reported. The analysis was based on the homonuclear ROESY, heteronuclear direct GHSQC, IDR‐GHSQC‐TOCSY, and long‐range GHMBC experiments. The complete ^1^H

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The synthesis of novel polycyclic heterocyclic ring systems via photocyclization. 21. Naphtho[2′,1′:4,5]thieno[2,3-c]naphtho[1,2-f]-quinoline, naphtho[2′,1′:4,5]thieno[2,3-c]naphtho[1,2-f][1,2,4]-triazolo[4,3-a]quinoline and naphtho[2′,1′:4,5]thieno[2,3-c]naphtho[1,2-f]-tetrazolo[1,5-a]quinoline
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## Abstract Photocyclization of 3‐chloro‐__N__‐(3‐phenanthryl)naphtho[1,2‐__b__]thiophene‐2‐carboxamide (**12**) furnished only one of the two possible isomers, __i.e.__, naphtho[2′,1′:4,5]thieno[2,3‐__c__]naphtho[1,2‐__f__]quinolin‐6(5__H__)‐one (**13**), which was further elaborated to yield the

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ChemInform Abstract: The Synthesis of Novel Polycyclic Heterocyclic Ring Systems via Photocyclization. Part 21. Naphtho[2′,1′:4,5]thieno[2,3-c]naphtho[1,2-f]quinoline, Naphtho[2′,1′:4,5]thieno[2,3-c]naphtho[1,2-f][1,2,4]triazolo [4,3-a]quinoline, and Naphtho[2′,1′:4,5]thieno[2,3-c]naphtho[1,2-f]tetrazolo[1,5-a]quinoline.
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## Abstract ChemInform is a weekly Abstracting Service, delivering concise information at a glance that was extracted from about 100 leading journals. To access a ChemInform Abstract of an article which was published elsewhere, please select a “Full Text” option. The original article is trackable v