Naphthalene-2,7-diol–1,2,4-triazole (2/1)
✍ Scribed by Wang, Yong-Tao ;Tang, Gui-Mei ;Ng, Seik Weng
- Publisher
- International Union of Crystallography
- Year
- 2006
- Tongue
- English
- Weight
- 158 KB
- Volume
- 62
- Category
- Article
- ISSN
- 1600-5368
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📜 SIMILAR VOLUMES
In the solid state, the structure of the title compound, C 10 H 8 O 2 , is stabilized by both van der Waals interactions and OÐHÁ Á ÁO intermolecular hydrogen bonds with OÁ Á ÁO distances of 2.714 (3) and 2.831 (4) A Ê .
## Abstract 2‐Amino‐1,2,3,4‐tetrahydronaphthalene‐6,7‐diol (**2**; 6,7‐ADTN) was synthesized starting from naphthalene‐2,3‐diol in seven steps and with an overall yield of 44%. Methylation of naphthalene‐2,3‐diol with dimethyl sulfate, followed by __Friedel____Crafts__ acylation with AcCl, gave 2‐
Amino-athylantinol-benzoesauremethylestcr (V) In eine iibersohiissiges Diazomethan enthaltende iitherische Losung werden portionsweise 3,8 g (20 mMol) IV eingetragen, das unter Stickstoffentwicklung in Losung geht. Man laat das Reaktionsgemisch 1 2 Stdn. bei Raumtemperatur stehen, filtriert und duns