N -Phenyl-4-(8-phenyl-4,5-dihydro-1,2-benzoxazolo[4,5- d ]thiazol-2-yl)piperidine-1-carboxamide
✍ Scribed by Hu, De-Jin; Liu, Ming; Huang, Tong-Hui; Tu, Hai-Yang; Zhang, Ai-dong
- Book ID
- 121838260
- Publisher
- International Union of Crystallography
- Year
- 2009
- Tongue
- English
- Weight
- 540 KB
- Volume
- 65
- Category
- Article
- ISSN
- 1600-5368
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📜 SIMILAR VOLUMES
All interatomic distances in the title compound, C~13~H~15~N~3~O~2~S, are normal. The 1,2,4-triazole ring is planar and is inclined at 46.50 (6)° to the phenyl ring. The ethoxycarbonylmethyl group is also close to being planar and is inclined at 87.54 (9)° to the 1,2,4-triazole ring. The crystal was
In the title complex, [Sn(C 6 H 5 ) 3 (C 8 H 7 N 4 S)], all bond lengths and angles show normal values. The Sn centre is fourcoordinated by three C atoms [Sn-C 2.119 (6)-2.133 (6) A ˚] and one N atom [Sn-N 2.107 (5) A ˚] in a distorted tetrahedral geometry. The crystal packing exhibits no classical
Single-crystal X-ray study T = 296 K Mean (C-C) = 0.005 A R factor = 0.054 wR factor = 0.151 Data-to-parameter ratio = 12.9 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.