N-(p-Nitrophenylsulfonyl)-1H-pyrrole
✍ Scribed by Gültekin, Zeynep ;Frey, Wolfgang ;Hökelek, Tuncer
- Publisher
- International Union of Crystallography
- Year
- 2004
- Tongue
- English
- Weight
- 228 KB
- Volume
- 60
- Category
- Article
- ISSN
- 1600-5368
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📜 SIMILAR VOLUMES
Single-crystal X-ray study T = 295 K Mean '(C±C) = 0.005 A Ê R factor = 0.050 wR factor = 0.206 Data-to-parameter ratio = 12.5 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
The title compound, C 11 H 10 BrNO 2 S, crystallizes in a columnar structure consisting of interdigitated CÐHÁ Á ÁO doubly bonded chains. The columns pack in a herring-bone fashion and are linked through additional weak hydrogen bonding. The structure is very nearly isomorphous to one in which the b
Single-crystal X-ray study T = 295 K Mean '(C±C) = 0.006 A Ê R factor = 0.040 wR factor = 0.123 Data-to-parameter ratio = 11.0 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
C 13 H 24 N 2 2O 2 Si, and 2,4-dinitropyrrole. In the solid state, the title compound exists as discrete molecules with only weak C-HÁ Á Ánitro hydrogen bonds between them.
In the title molecule, C 21 H 17 NO 3 S 2 , the sulfonyl-bound and sulfinyl-bound phenyl rings form dihedral angles of 82.04 (5) and 26.26 (8) , respectively, with the indole ring system. In the crystal structure C-HÁ Á ÁO, C-HÁ Á Á andinteractions form a two-dimensional network.