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N-Butyl-4-butylamino-1,8-naphthalimide

✍ Scribed by Banthia, Sandip (author);Paul, Aniruddha (author)

Publisher
International Union of Crystallography (IUCr)
Year
2005
Tongue
English
Weight
162 KB
Volume
61
Category
Article
ISSN
1600-5368

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📜 SIMILAR VOLUMES

N -Butyl-4-butylamino-1,8-naphthalimide
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Single-crystal X-ray study T = 163 K Mean '(C±C) = 0.005 A Ê R factor = 0.045 wR factor = 0.090 Data-to-parameter ratio = 12.6 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

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Single-crystal X-ray study T = 90 K Mean '(C±C) = 0.002 A Ê R factor = 0.038 wR factor = 0.100 Data-to-parameter ratio = 14.0 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

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The title compound, C 19 H 12 N 2 O 3 , was prepared by the reaction of hydrazine and salicylaldehyde with 1,8-naphthoic anhydride in refluxing dimethylformamide. The structure is stabilized by an intramolecular O-HÁ Á ÁN hydrogen bond and the crystal packing exhibits C-HÁ Á ÁO hydrogen bonds. The d