Single-crystal X-ray study T = 90 K Mean '(C±C) = 0.002 A Ê R factor = 0.038 wR factor = 0.100 Data-to-parameter ratio = 14.0 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
N-(2-Hydroxybenzylideneamino)-1,8-naphthalimide
✍ Scribed by Jian, Fang-Fang ;Du, Li ;Yi, Wei
- Publisher
- International Union of Crystallography
- Year
- 2007
- Tongue
- English
- Weight
- 301 KB
- Volume
- 63
- Category
- Article
- ISSN
- 1600-5368
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✦ Synopsis
The title compound, C 19 H 12 N 2 O 3 , was prepared by the reaction of hydrazine and salicylaldehyde with 1,8-naphthoic anhydride in refluxing dimethylformamide. The structure is stabilized by an intramolecular O-HÁ Á ÁN hydrogen bond and the crystal packing exhibits C-HÁ Á ÁO hydrogen bonds. The dihedral angle formed by the benzene and naphthalimide systems is 175.9 .
📜 SIMILAR VOLUMES
Single-crystal X-ray study T = 163 K Mean '(C±C) = 0.005 A Ê R factor = 0.045 wR factor = 0.090 Data-to-parameter ratio = 12.6 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.