Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.005 A Ê R factor = 0.053 wR factor = 0.167 Data-to-parameter ratio = 15.4 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
N-Benzyl-2-methylfuran-3-thiocarboxanilide
✍ Scribed by Pavlović, Gordana ;Tralić-Kulenović, Vesna ;Popović, Zora
- Book ID
- 104481703
- Publisher
- International Union of Crystallography
- Year
- 2004
- Tongue
- English
- Weight
- 255 KB
- Volume
- 60
- Category
- Article
- ISSN
- 1600-5368
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📜 SIMILAR VOLUMES
The dihedral angle between the benzoyl and benzyl groups in the title compound, C 16 H 16 N 2 OS, is 63.63 (4) . The crystal packing is characterized by N-HÁ Á ÁO and N-HÁ Á ÁS hydrogen bonds.
Single-crystal X-ray study T = 296 K Mean '(C±C) = 0.003 A Ê R factor = 0.044 wR factor = 0.120 Data-to-parameter ratio = 13.9 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
A simple and convenient method for the microsynthesis of tritiated 3-methylfuran and trttiated 2-1nethylfuran froa 3furfuryl chloride and 2-furfuryl chloride, respectively, has been described. The tritium label was introduced by reductive dehalogenation with tritiated lithim aluminum hydride.
The title compound, [Zn(C 12 H 10 N 2 O 2 S) 2 (C 2 H 6 OS)], is monomeric with the Zn atom in a ®ve-coordinate environment. The geometry of the polyhedron is distorted trigonal bipyramidal, with angles of the equatorial atoms about the central Zn atom in the range 77.84 (10)±126.66 (12) A Ê . The O