N-(4-Chlorobenzyl)phthalimide
✍ Scribed by Chen, Ping ;Li, Dan ;Zhang, Ling
- Publisher
- International Union of Crystallography
- Year
- 2006
- Tongue
- English
- Weight
- 174 KB
- Volume
- 62
- Category
- Article
- ISSN
- 1600-5368
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The title compound, C 16 H 13 NO 2 , was synthesized by Nalkylation of 4-methylbenzyl bromide with phthalimide. The phthalimide ring system is essentially planar and forms a dihedral angle with the tolyl ring of 69.5 (6) .
In the title compound, C~15~H~9~Cl~2~NO~2~, the dihedral angle between the phthalimide ring system and the dichlorobenzene ring is 93.5 (4)°.
In the title compound, C~23~H~27~NO~3~, the molecules are held together by intermolecular C—H...O hydrogen bonds and π–π stacking interactions.
Single-crystal X-ray study T = 273 K Mean '(C±C) = 0.003 A Ê R factor = 0.040 wR factor = 0.112 Data-to-parameter ratio = 17.1 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
In the title compound, C 15 H 11 NO 2 S, the dihedral angle between the two planar ring systems is 74.49 (5) .