✦ LIBER ✦

N-(4-Bromobenzylidene)-4-methoxyaniline

✍ Scribed by Ma, Rui ;Hou, Yubang ;Yong, Xuejian ;Cen, Yunbin

Book ID: 104491802
Publisher: International Union of Crystallography
Year: 2007
Tongue: English
Weight: 416 KB
Volume: 63
Category: Article
ISSN: 1600-5368
DOI: 10.1107/s1600536807046855

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✦ Synopsis

In the title compound, C 14 H 12 BrNO, the torsion angle about the central C N double bond is 170.4 (3) and the dihedral angle between the aromatic rings is 9.6 (3) .

Related literature

For related literature, see: Gao et al. (2004); Sun et al. (2006). Experimental Crystal data C 14 H 12 BrNO M r = 290.15 Orthorhombic, Pca2 1 a = 6.1510 (8) A b = 7.2726 (9) A c = 27.914 (4) A ˚V = 1248.7 (3) A ˚3 Z = 4 Mo K radiation = 3.27 mm À1 T = 292 (2) K 0.10 Â 0.10 Â 0.06 mm Data collection Bruker SMART CCD diffractometer Absorption correction: multi-scan (SADABS; Bruker, 1997) T min = 0.728, T max = 0.822 8336 measured reflections 2349 independent reflections 1512 reflections with I > 2(I) R int = 0.063 Refinement R[F 2 > 2(F 2 )] = 0.064 wR(F 2

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