𝔖 Bobbio Scriptorium
✦   LIBER   ✦

N-(3-Chloro­phen­yl)-2-cyano-3-(4-hydr­oxy-3-meth­oxy-2-nitro­phen­yl)prop-2-enamide

✍ Scribed by Zheng, Xian-Ming ;Hu, Wei-Xiao ;Xu, Feng

Publisher
International Union of Crystallography
Year
2007
Tongue
English
Weight
257 KB
Volume
63
Category
Article
ISSN
1600-5368

No coin nor oath required. For personal study only.

✦ Synopsis

In the title compound, C~17~H~12~ClN~3~O~5~, the benzene rings are twisted out of the central –C~ar~–C–C(–CN)–C(=O)–N–plane. The dihedral angles between this plane and the aromatic planes are 31.2 (4) and 4.8 (3)°. The C=C double bond is in an E configuration.

📜 SIMILAR VOLUMES

3-(4-Hydr­oxy-3-meth­oxy-2-nitro­phen­yl
3-(4-Hydr­oxy-3-meth­oxy-2-nitro­phen­yl)acrylic acid
✍ Xia, Chun-Nian ;Hu, Wei-Xiao ;Zhou, Wei 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 86 KB

Single-crystal X-ray study T = 298 K Mean (C-C) = 0.006 A Disorder in main residue R factor = 0.095 wR factor = 0.243 Data-to-parameter ratio = 12.2 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

(3-Chloro­phen­yl)(2-hydr­oxy-5-methyl­p
(3-Chloro­phen­yl)(2-hydr­oxy-5-methyl­phen­yl)methanone
✍ Khanum, S. A. ;Mahendra, M. ;Shashikanth, S. ;Doreswamy, B. H. ;Sridhar, M. A. ; 📂 Article 📅 2005 🏛 International Union of Crystallography 🌐 English ⚖ 246 KB

In the title compound, C 15 H 14 ClO 2 , the dihedral angle between the two benzene rings is 57.37 (12) .

2-{[2-Chloro-5-(4-methoxy­phen­yl)pyridi
2-{[2-Chloro-5-(4-methoxy­phen­yl)pyridin-3-yl](hydr­oxy)meth­yl}acrylonitrile
✍ Swamy, G. Y. S. K. ;Ravikumar, K. ;Narender, P. ;Rao, V. Jayathirtha 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 220 KB

In the title compound, C 16 H 13 ClN 2 O 2 , the dihedral angle between the pyridine and benzene rings is 40.1 (1) . There is a weak intramolecular C-HÁ Á ÁCl interaction. Molecules are linked via O-HÁ Á ÁN hydrogen bonds, forming chains of graph-set motif C(6) along the a axis.

N-[4-Cyano-3-(trifluoro­meth­yl)phen­yl]
N-[4-Cyano-3-(trifluoro­meth­yl)phen­yl]-3-(4-fluoro­phenyl­sulfan­yl)-2-hydr­oxy-2-methyl­propionamide
✍ Hu, Xiu-Rong ;Wang, Li-Li ;Gu, Jian-Ming 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 201 KB

Single-crystal X-ray study T = 296 K Mean (C-C) = 0.004 A Disorder in main residue R factor = 0.065 wR factor = 0.175 Data-to-parameter ratio = 16.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

N-[4-Cyano-3-(trifluoro­meth­yl)phen­yl]
N-[4-Cyano-3-(trifluoro­meth­yl)phen­yl]-3-(4-fluoro­phenyl­sulfon­yl)-2-hydr­oxy-2-methyl­propionamide
✍ Hu, Xiu-Rong ;Gu, Jian-Ming 📂 Article 📅 2005 🏛 International Union of Crystallography 🌐 English ⚖ 254 KB

The structure of the title compound, C 18 H 14 F 4 N 2 O 2 S, consists of molecules that pack in a linear hydrogen-bonded chain along the c axis. This hydrogen-bonding arrangement involves the hydroxy group and one of the sulfonyl O atoms.