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Mössbauer and ESR study of pyridine-inactive phthalocyanineiron (II) in zeolite supercage

✍ Scribed by M. Tanaka; Y. Minai; T. Watanabe; T. Tominaga

Book ID
112706981
Publisher
Springer
Year
1991
Tongue
English
Weight
394 KB
Volume
154
Category
Article
ISSN
1588-2780

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## Phthalocyanineiron(I1) (FePc) was synthesized in FeY zeolite supercage with acid sites. Miissbauer spectroscopy was employed to determine the yield of FePc(py), produced by contact of FePc with pyridine in it. Although the supercage had enough space to form FePc(py),, the yield was very low. Th

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The ESR technique has been used to study the localization of copper@) ions in the zeoijte framework. In the enti@y hydrated samples the copper(H) ion is in the form of an hexazquo complex localized in the centre of the supercage. Dehydration produces the migration qf the ion toward the sodalite cage