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Multistep Redoxsystems, LX. 1,4,5,8-Tetraoxo-1,4,5,8-tetrahydrothianthrene: Synthesis, Structure, and Spectroelectrochemical Properties

✍ Scribed by Hünig, Siegfried ;Sinzger, Klaus ;Bau, Robert ;Metzenthin, Tobias ;Salbeck, Josef

Book ID
118282731
Publisher
Wiley (John Wiley & Sons)
Year
1993
Tongue
English
Weight
681 KB
Volume
126
Category
Article
ISSN
0009-2940

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To a cold (-78'C) solution of 10 mmoles of the iithium derivative ( I ) , RI=CH3, in tetrahydrofuran 111 was added with stirring 1.06 g (10 mmoles) of benzonitrile. The resulting bright orange mixture was kept at -78 O C for 40 min, after which the bath was removed and stirring was continued for an