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Multipolymer-Supported Substrate and Ligand Approach to the Sharpless Asymmetric Dihydroxylation

✍ Scribed by Dr. Hyunsoo Han; Prof. Kim D. Janda

Publisher
John Wiley and Sons
Year
1997
Tongue
English
Weight
396 KB
Volume
36
Category
Article
ISSN
0044-8249

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✦ Synopsis

followed except acetone'water iis solvent and NMO were used. The reaction mixture contained a small amount of OsO, in t-BuOH (2.5% solution. 13 pL, 0.01 equiv based on olefin), the ligand (0.0025 g, 0.025 equiv), N M O (0.022 g, 1.5 equiv), and tetraethylammonium acetate tetrahydrate (0.033 g, 1 0 equiv) in acetoneiwater (4 mL, 10/1 v/v) at 4 'C

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