Monitoring the hydrothermal precipitation of α-Fe2O3 from concentrated Fe(NO3)3 solutions partially neutralized with NaOH
✍ Scribed by Mark Žic; Mira Ristić; Svetozar Musić
- Book ID
- 108213322
- Publisher
- Elsevier Science
- Year
- 2011
- Tongue
- English
- Weight
- 891 KB
- Volume
- 993
- Category
- Article
- ISSN
- 0022-2860
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Different alcohols were formylated by formic acid under solvent-free conditions in the presence of iodine as the catalyst with good-to-high yields at room temperature. I 2 generated in situ from Fe(NO 3 ) 3 •9H 2 O/NaI also catalyzed the formylation of the alcohols under solvent-free conditions. Thi
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## Abstract Structurally diverse alcohols and phenols were trimethylsilylated in a clean and efficient reaction with hexamethyldisilazane (HMDS) based on the use of I~2~ generated __in situ__ from Fe(NO~3~)~3~⋅9 H~2~O/NaI. The reaction occurs very rapid in good‐to‐high yield in CH~2~Cl~2~ at room t