Molecular structure of the s-triazine-Br2 complex
β Scribed by Mark Mascal; John L. Richardson; Alexander J. Blake; Wan-Sheung Li
- Publisher
- Elsevier Science
- Year
- 1996
- Tongue
- French
- Weight
- 112 KB
- Volume
- 37
- Category
- Article
- ISSN
- 0040-4039
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## Abstract Functionalised dialkoxyβsubstituted tetraoxacalix[2]arene[2]triazine macrocycles **6** have been readily synthesised by the fragment coupling approach using methyl 3,5βdihydroxyβ4βalkoxybenzoates and cyanuric chloride as the starting materials under very mild conditions. AlCl~3~βmediate
An anion (loss of 3N hydrogen) of a 2-acetylpyridine azacyclothiosemicarbazone coordinates in a planar conformation to the central Cu atom through the pyridyl N, azomethine N and thiolato S atoms. The interatomic distances are Cu--N = 2.016( 6), Cu--N = 1.963( 5) and Cu--S=2.236(3)~, respectively, w