Molecular structure of 1-phenyl-1-dimethylamino-4,4-bis(trimethylsilyl)-2-aza-3λ3-phosphabutadiene-1,3
✍ Scribed by Alexander N. Chernega; Eduard B. Rusanov; Mark I. Povolotskii
- Book ID
- 110274958
- Publisher
- Springer
- Year
- 1999
- Tongue
- English
- Weight
- 112 KB
- Volume
- 29
- Category
- Article
- ISSN
- 1572-8854
No coin nor oath required. For personal study only.
📜 SIMILAR VOLUMES
I ,I ,3,3 -Tetrakis(dimethylamin0) -1 h5,3h5diphosphete, 1, reacts with cyanoformic acid methyl ester to form two isomers of the title compound 2. Properties, NMR, mass, and IR spectra of 2, as well as the molecular and crystal structure of the E isomer of 2, are described and discussed.
supplementary materials sup-2 (0.01 mol) in methanol (30 ml), and 3, 4-dimethoxyacetophenone (0.01 mol) in methanol (30 ml). Single crystals of the title compound suitable for X-ray analysis were grown by slow evaporation of an acetone solution at room temperature. ## Refinement All H atoms were