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Molecular modelling and chemical synthesis of molecular ‘mappemondes’ designed from a calix[4]-bis-crown

✍ Scribed by Zouhair Asfari; Christoph Naumann; Gérard Kaufmann; Jacques Vicens

Publisher
Elsevier Science
Year
1996
Tongue
French
Weight
200 KB
Volume
37
Category
Article
ISSN
0040-4039

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📜 SIMILAR VOLUMES

Synthesis of a molecular mill designed f
Synthesis of a molecular mill designed from a calix[4]-bis-crown
✍ Zouhair Asfari; Christoph Naumann; Gérard Kaufmann; Jacques Vicens 📂 Article 📅 1998 🏛 Elsevier Science 🌐 French ⚖ 194 KB

The synthesis of molecular mill 4 has been achieved by condensing the dibromomethyl derivative of a calix[4]-bis-crown 1 with naphtho polyether diol 2 in high dilution conditions.

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Hydrosoluble Calix[4] arenes-bis-crown-6 2a, 3a and 3b have been synthesised in two steps via formylation and chlorosulfonylation of 1. Cs +-Ligand interactions were studied in aqueous media by UV-Visible analysis and showed a good affinity between receptor 2a and the caesium ion.

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