Alkaline hydrolysis of various orgamc sulphur compounds (thioacetamide, thiosemicarbazide, thiodiacetic acid and dithiooxamide) in a continuous-flow analyzer produces sulphide which can be removed from the solution after acidification. Hydrogen sulphide evolved is measured by molecular emission cavi
โฆ LIBER โฆ
Molecular emission cavity analysis for organic sulphur compounds after electrolytic generation of hydrogen sulphide
โ Scribed by N. Grekas; A.C. Calokerinos
- Book ID
- 104100341
- Publisher
- Elsevier Science
- Year
- 1987
- Tongue
- English
- Weight
- 407 KB
- Volume
- 202
- Category
- Article
- ISSN
- 0003-2670
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โฆ Synopsis
Organic sulphur compounds (thiosemicarbaxide and dithioxamide) are determined in the range 5.00-30.0 m ml-'. Electrolysis is done between two platinum electrodes in a closed vapour-generation system. Various parameters which affect the procedure are investigated in detail. Other sulphur-containing compounds can be determined with different sensitivities.
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