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Molecular complexes of acetylene alcohols with n- and χ-donors

✍ Scribed by Fumio Toda; Katsuhiko Akagi

Publisher
Elsevier Science
Year
1968
Tongue
French
Weight
171 KB
Volume
9
Category
Article
ISSN
0040-4039

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✦ Synopsis

In the course of study on acetylene alcohols we have found that 1,1,6,&tetraphenylhexa-2,&.-diyne-1,6-diol (Ia) and 1,1,.!+,4-tetraphenylbut-2-yne-l,&-diol (IIa) formed crystalline * complexes with various n-endkdonors by definite ratio. The most interesting complexes were derived from Ia and haloalksnes such as carbon tetrachloride, chloroform and methylene chloride.

Infrared spectra showed that the complexes have strong hydrogen-bonding.

Among eight kinds of acetylene alcohols tested, tetraphenyl di and monoacetylene diols

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