The effect of dipolar coupling to 14 N on 13 C FIREMAT ( five π replicated magic angle turning) experiments is investigated. A method is developed for fitting the 13 C FIREMAT FID employing the full theory to extract the 13 C-14 N dipolar and 13 C chemical shift tensor information. The analysis requ
✦ LIBER ✦
Molecular and structural information from variable-angle spinning NMR dipolar spectra of 13C-14N systems
✍ Scribed by Zhehong Gan; David M Grant
- Publisher
- Elsevier Science
- Year
- 1990
- Weight
- 771 KB
- Volume
- 90
- Category
- Article
- ISSN
- 0022-2364
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## Abstract It is demonstrated that in a case where neither the proton nor the natural‐abundance ^13^C‐satellite spectra of a partially oriented molecule carry enough structural information, one can determine the entire molecular geometry by the combined use of several liquid crystals as solvents.