Both 13C-and 15N-REDOR experiments were performed to determine the '3C-'5N interatomic distance in [ I-"C]N-acetyl-Pro-[ '5N]GIy-Phe crystal and to evaluate the inter-or intra-molecular dipolar contributions leading to its errors. The interatomic distance was determined to be 3.43 8, after removing
✦ LIBER ✦
A simple approach for relating molecular and structural information to the dipolar coupling 13C14N in CPMAS NMR
✍ Scribed by Alejandro C Olivieri; Lucid Frydman; Luis E Diaz
- Publisher
- Elsevier Science
- Year
- 1987
- Weight
- 738 KB
- Volume
- 75
- Category
- Article
- ISSN
- 0022-2364
No coin nor oath required. For personal study only.
📜 SIMILAR VOLUMES
Inter- and intra-molecular contributions
✍
A. Naito; K. Nishimura; S. Tuzi; H. Saitô
📂
Article
📅
1994
🏛
Elsevier Science
🌐
English
⚖ 475 KB
The rα-structure of partially oriented 1
✍
G. Dombi; J. Amrein; P. Diehl
📂
Article
📅
1980
🏛
John Wiley and Sons
🌐
English
⚖ 322 KB
## Abstract It is demonstrated that in a case where neither the proton nor the natural‐abundance ^13^C‐satellite spectra of a partially oriented molecule carry enough structural information, one can determine the entire molecular geometry by the combined use of several liquid crystals as solvents.