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Molecular and crystal structures of 2,3,4,6,1′,3′,4′,6′-octa-O-acetyl-β-sophorose, methyl 2,3,4,6,3′,4′,6′-hepta-O-acetyl-β-sophoroside, and methyl 2,3,4,6,3′,4′-hexa-O-acetyl-6′-deoxy-β-sophoroside

✍ Scribed by Masaki Ikegami; Tomoya Sato; Kouichi Suzuki; Keiichi Noguchi; Kenji Okuyama; Shinichi Kitamura; Kenichi Takeo; Shigeru Ohno

Publisher: Elsevier Science
Year: 1995
Tongue: English
Weight: 639 KB
Volume: 271
Category: Article
ISSN: 0008-6215
DOI: 10.1016/0008-6215(95)00093-9

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✦ Synopsis

The molecular and crystal structures of 2, 3,4,6,1',3',4',6'-octa-O-acetyl-fl-sophorose (flsophorose octaacetate), methyl 2,3,4,6,3',4',6'-hepta-O-acetyl-/3-sophoroside (methyl /3-sophoroside heptaacetate), and methyl 2,3,4,6,3',4'-hexa-O-acetyl-6'-deoxy-fl-sophoroside (methyl 6'-deoxy-fl-sophoroside hexaacetate) were determined by X-ray diffraction. All structures were obtained by the direct method and refined by the full-matrix least-squares procedure. The crystal data and final R values are as follows: /3-sophorose octaacetate, C28019H38, monoclinic, P21,

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