a Reagents used in equimolar amounts (entries 4ยฑ6) or in excess of diene, 5/1 (entries 2, 3), 3/1 (entry 7), 2/1 (entry 1) b Yield of isolated product relative to the minor reagent. c Sequential MW irradiation (SMWI); applied incident power; time and number of irradiations; interval between two irra
Microwaves in Organic Synthesis Volume 6 || Microwave-assisted Reactions on Graphite
โ Scribed by Loupy, Andr
- Book ID
- 111674831
- Publisher
- Wiley-VCH Verlag GmbH
- Year
- 2006
- Tongue
- German
- Weight
- 935 KB
- Edition
- 2nd, Completely Revised and Enlarged
- Category
- Article
- ISBN
- 3527314520
No coin nor oath required. For personal study only.
โฆ Synopsis
The long awaited new edition of this comprehensive two-volume reference has been completely updated and expanded by 30% to include chapters on ionic liquids, carbohydrate chemistry, multicomponent reactions, solid phase peptide synthesis, carbon nanotubes and fullerenes. Written by the most eminent scientists in their respective fields, the chapters, which complement one another, now also include eight new fields of application, such as heterocyclic chemistry, cycloadditions and carbohydrate chemistry. In addition, very promising techniques under development are treated, resulting from the application of microwave irradiation to combinatorial chemistry, radiochemistry and photochemistry.
The standard reference in this booming field.
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## Abstract The coupling of graphite (as a support) with microwaves (as an energy source), a new type of โdry reactionโ, was studied for some DielsโAlder reactions involving anthracene and azadienes. Graphite is responsible for a highโtemperature gradient leading to increased reaction rates as comp